| Device / Manufacturer (Country) |
|
Description of the Experiment or Analysis |
Made |
Service |
| Gas chromatograph with flame ionization detector, mass spectrometry detector, and Agilent H2-GC/FID, MSD, SCD sulfur chemiluminescence detector / Agilent Technolgies, Inc. (USA) |
|
The analyses allow for parallel quantitative analysis with the FID detector and the SCD sulfur detector, and qualitative and semi-quantitative analysis with the MSD detector |
2022 |
Kaluža |
| Automatic Physisorption Analyzer ASAP 2020 / Micromeritics Instrument Corp. (USA) |
|
Determination of specific surface area, total pore volume, micro- and mesopore size distribution from N2 (77 K) and Ar (87 K) adsorption isotherms. Determination of specific surface area from Kr (77 K) adsorption isotherm for low surface area materials (< 1 m2 g-1) |
2006 |
Soukup |
| Automatic Physisorption Analyzer ASAP 2050 / Micromeritics Instrument Corp. (USA) |
|
Determination of specific surface area, total pore volume, and mesopore size distribution from the N2 (77 K) adsorption isotherm. Determination of mesopore distribution from theCO2 (273 K) adsorption isotherm. Determination of high-pressure (up to 1000 kPa) CO2 and H2 isotherms over a wide temperature range from 77 K to 353 K |
2009 |
Soukup |
| Autosorb iQ-C-XR PFE combined physisorption and chemisorption analyzer / Quantachrome Instruments (USA) |
|
Determination of the specific surface area, total pore volume, micro- and mesopore size distribution from adsorption isotherms of N2 (77 K) and Ar (87 K). Determination of the specific surface area from adsorption isotherm Kr (77 K) and pore size distribution from adsorption isotherm Kr (87 K) for low surface area materials (< 1 m2 g-1). Determination of the physisorption and chemisorption of a range of gases including e.g. CH4, H2, CO, CO2, NH3, N2O |
2022 |
Soukup |
| Mercury Porosimeter AutoPore IV 9520 / Micromeritics Instrument Corp. (USA) |
|
Determination of specific intrusion volume, apparent density, meso- and macropore size distribution (up to approx. 360 mm diameter), and tortuosity in porous materials |
2014 |
Soukup |
| Helium pycnometer AccuPyc II 1340 / Micromeritics Instrument Corp. (USA) |
|
Determination of the true (skeletal) density of solid samples |
2012 |
Soukup |
| Chemisorption with MS Omnistar / Micromeritics Instrument Corp. and Pfeiffer Vacuum (USA) |
|
Chemisorption, temperature-programmed reactions |
2011 |
Kaluža |
| Physisorption Analyzer, FlowSorb III / Micromeritics Instrument Corp. (USA) |
|
Nelsen-Eggertsen flow physisorption of nitrogen (measurement of the specific surface area of unstable samples) |
2002 |
Kaluža |
| Graham diffusion cell |
|
Counter-current diffusion of gases under laboratory pressure |
|
Soukup |
| Inverse Gas Chromatography |
|
Diffusion of gases in solids |
|
Soukup |
| Inverse liquid chromatography |
|
Diffusion of liquids in solids |
|
Soukup |
| Liquid Displacement Permporometry |
|
Transport pore size distribution |
|
Soukup |
| Permeation cell |
|
Permeation of gases in solids |
|
Soukup |
| Hydrogenation, oxidation, and TPR/TPD apparatuses |
|
Measurement of activity and reducibility, basicity and acidity of catalysts |
|
Topka Kaluža |
| Photocatalytic reactors |
|
Measurement of photocatalytic activity, decontamination |
|
Dlasková |
| Wicke-Kallenbach diffusion cell |
|
Countercurrent diffusion of gases under reduced pressure |
|
Soukup |
| Batch stainless-steel high-pressure reactor / Büchi Labortechnik AG (Switzerland) |
|
Autoclave with a volume of 250 cm3 up to a working pressure of max. 60 bar and a temperature of 250 °C |
2010 |
Soukup |
| Laboratory equipment for preparation of nanofibrous formations by electrostatic softening technique / Cersum s.r.o. (CR) |
|
Preparation of nanofibrous formations (catalyst supports and membranes) with a nanofibre diameter distribution of 50 – 750 nm based on a wide range of polymers |
2012 |
Balabánová |
| Annealing flow furnace, model Carbolite / Keison Intern. Ltd. (UK) |
|
Annealing of solid samples (more than 50 ml) |
2010 |
Jirátová |
| Annealing crucible furnace up to 1000 °C |
|
Annealing of solid samples |
1990 |
Jirátová |
| Laboratory kneader 150 ml, / Fritsch GmbH – Milling and Sizing (Germany) |
|
Preparation of solid pastes |
2011 |
Balabánová Kaluža |
| Laboratory planetary mill / Fritsch GmbH – Milling and Sizing (Germany) |
|
Grinding of solid samples, preparation of pastes |
2014 |
Kaluža |
| Tubular reactor for catalytic oxidation of VOCs equipped with GC-MS Agilent 8890 / Agilent Technologies (USA) |
|
Total catalytic oxidation of volatile organic compounds (VOC) |
2020 |
Topka |
| Gas analyzer, Ultramat 23 / Siemens (Germany) |
|
Determination of CO and CO2 concentrations |
2000 |
Jirátová |
| Tubular catalytic reactors |
|
Measurement of activities and selectivities of solid catalysts in C-C condensation reactions (Guerbet, ketonization) |
|
Kaluža |
| Calcination furnace up to 1200 °C |
|
Annealing of solid samples |
2013 |
Dlasková |
| Coating box |
|
Preparation of thin films, dip coating |
2007 |
Dlasková |
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